Optimized Pinhole Geometry for Small-Angle Scattering

TitleOptimized Pinhole Geometry for Small-Angle Scattering
Publication TypeJournal Article
Year of Publication2015
AuthorsWacha, A
JournalJournal of Applied Crystallography
Volume48
Issue6
Start Page1843
Pagination1843–1848
Date Published10/2015
ISSN1600-5767
KeywordsCREDO
Abstract

In order to make the most from the low photon flux in laboratory small-angle X-ray scattering instruments, the experimental geometry has to be chosen carefully, with special stress on the beam-shaping system. The optimum collimation scheme should enable accurate measurements over the desired range of the scattering variable, while yielding the highest flux and the lowest possible instrumental background. In order to identify the best setting, a phase-space optimization of the collimating scheme is carried out in the present work, including constraints on the beam size at the sample position and on the detector surface. The resulting formulae are implemented in a Python script with a graphical user interface, to aid the planning, construction and daily operation of pinhole small-angle scattering cameras.

DOI10.1107/S1600576715018932
Refereed DesignationRefereed